Fmoc-D-Cyclohexyl glycine（CAS# 198543-96-3)

Āhuatanga matū:

Tātai rāpoi	C23H25NO4
Molar Mass	379.45
Kiato	1.238
Te Whakarewa	161-187 ℃
Piro Pouri	602.9±38.0 °C(I Matapaetia)
Te ahua	Ma ki te paura ma
pKa	3.89±0.10(I Matapaetia)
Tikanga Rokiroki	I hiri ki te maroke, Te Pawera o te rūma

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Fmoc-D-Cyclohexyl glycine（CAS# 198543-96-3) Nga korero

Whakamahi

Ko te Fluorene methoxycarbonyl D-cyclohexylglycine he takawaenga rongoa me te matū, ko te fluorenyl chloride (FMOC-Cl) he chloroformate. Ka whakamahia hei hanga i te fluorene methoxycarbonyl (rōpū FMOC) ki roto i te fluorene methoxycarbonyl carbamate FMOC carbamate, he roopu tiaki amino noa.

Whakaritenga

Ko te whakahiato o te fluorene methoxycarbonyl D-cyclohexylglycine kua korerohia i roto i nga tuhinga. Ma te whakamahi i te cyclohexyl bromide hei rauemi mata, i te aroaro o te konutai alkoxide, ka uru ki te tauhohenga alkylation ki te diethyl malonate, katahi ka whakamaarama, ka waikawa, ka decarboxylates kia whiwhi ai i te waikawa cyclohexyl acetic; ka brominated te whakamutunga me te ammonolysis DL-Cyclohexylglycine; ka mutu, ka puta te tauhohenga acylation i te aroaro o te fluorene methoxycarbonyl chloride ki te whiwhi fluorene methoxycarbonyl D-cyclohexylglycine [1]. Ko te ara tauhohenga whakahiato e whai ake nei:

Tōmua: AC-TYR-NH2（CAS# 1948-71-6)

Panuku: 2-Amino-4-bromobenzoic acid（CAS# 20776-50-5)

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