Lomefloxacin hydrochloride CAS 98079-52-8
Morearea me te Haumaru
| Nga Tohu Whakamate | Xn – He kino |
| Waehere Morearea | 22 – He kino ki te horomia |
| WGK Tiamana | 3 |
| RTECS | VB1997500 |
| Waehere HS | 29339900 |
Te whakatau ihirangi
Raraunga Whaimana kua Manatokohia
ka inehia e te chromatography wai mahi teitei (General 0512).
tikanga chromatographic me te whakamatautau pai o te punaha
ko te silica gel kua herea ki te octylsilane hei whakakii; Wairewa konutai pentanesulfonate (konutai pentanesulfonate 1.5g, haukinia dihydrogen phosphate 3.0g, wai 950ml ki te tareka, whakarite pH ki ki te waikawa ūkuikui, waimeha ki te 1000ml ki te wai)-Methanol (65:35) rite wāhanga pūkoro, tere rere o 1.2ml ia meneti, kitea te roangaru o te 287mn. Tangohia te otinga e pa ana ki te punaha 20u1 i raro i te taonga o nga matū e pa ana, ka werohia ki roto ki te Liquid Chromatograph tangata. Ko te wa pupuri o te lomefloxacin e tata ana ki te 9 meneti, me te tohu wehenga i waenga i te tihi poke i te wa pupuri whanaunga tata ki te 0.8 me te tihi o te lomefloxacin kia nui ake i te 2.0, ko te whakatau i waenga i te tihi o te lomefloxacin me te tihi poke i te wa pupuri whanaunga 1.1 kia tutuki nga whakaritenga.
whakamātautau
tangohia te nui tika o tenei hua, te pauna tika, me te whakakore i te wahanga pūkoro me te waimeha ine i mahia i roto i ia lml kei roto mo te 0. I whakamahia te otinga lmg hei otinga whakamatautau, a ka werohia te 20ul ki roto i te chromatograph wai me te tika, me te chromatogram i tuhia. Ko tetahi atu matū tohutoro lomefloxacin i tangohia ka whakatauhia ma te tikanga ano. Ko te ihirangi o te lomefloxacin (C17H19F2N303) i roto i te tauira i tatauhia e te waahi teitei i runga i te tikanga paerewa o waho.
